by Denise Sullivan Denise Sullivan No Comments

HPLC Spring Energized Seals

HPLC spring energized seals

High-performance liquid chromatography is the ideal method for analyzing various solutions in different fields. This machine, however, requires HPLC spring energized seals that adhere to strict guidelines with slight variation.

Different Liquid Chromatography Types

There are a few different types of liquid chromatography. The primary liquid chromatography types include high-performance liquid chromatography (HPLC), preparative HPLC, and ultra-high-performance liquid chromatography.

High-performance liquid chromatography is used in multiple different industries. HPLC is found in food science, drug development, and forensic analysis. It is used to separate compounds and used for quantitative and qualitative analysis.

Preparative HPLC is used in purification applications as it requires a higher flow rate. This liquid chromatography is also used to separate and collect high-purity compounds. It is also used for large quantities of compounds needed for evaluation and analysis.

Ultra-high-performance liquid chromatography (UHPLC) is similar to HPLC. It is used to separate different constituents of a compound and to identify and quantify the different components of a mixture. 

Operating Conditions

HPLC pumps operate in conditions with variable flow rates and small shaft diameters. They have tight leak criteria and operate under a wide range of pressures. HPLC pumps have a medium-speed reciprocation.

Seals in HPLC pumps must withstand the solvents used to separate compounds dissolved in the liquid sample. Solvents used in HPLC include 

  • MeOH (Methanol)
  • ACN (Acetonitrile)
  • H2O (Water).

The expected lifetime for seals in HPLC pump environments is a minimum of one million cycles. Seals may last longer depending on the flow rate, pressure, and media.

Seal Designs

HPLC seals prevent leaks from occurring. Should the mile phase lack into the back of the pump, it will impact consistency, accuracy, and pump precision. To effectively prevent leaks, seals should have effective leak resistance in pressures up to 20 kpsi.

Seal Geometry

The geometry of the seal is an important factor. For HPLC pumps, a flange design helps reduce the pump’s pulsation. HPLC spring energized seals have a longer seal ID lip and a polymer backup ring to increase the amount of contact stress.

UHPLC seals have a non-flange design and a shorter seal ID lip. Instead of a polymer backup ring, it uses a ceramic or metal backup ring. These seals have a concave back for higher-pressure distribution.

Jacket Materials

HPLC pumps’ seals have a PTFE or UHMW PE jacket. The UHMW PE material is used in systems with pressures greater than ten kpsi. UHMW PE is an FDA-compatible material for both food and pharmaceutical analysis.

PTFE jackets are the most chemical resistant of the common materials. The PTFE jackets are filled with graphite or polyimide. These fillers are heat and wear-resistant and work well in liquids and steam.

Performance Factors

Sealing performance factors are affected by the different surfaces in the HPLC pump. The housing surface has a suggested static sealing surface between 9.1 to 14.5 μin Ra.

On the plunger surface, a smoother surface is best. For virgin PTFE or UHMW PE, a minimum shaft hardness is 40Rc. The suggested dynamic surface is 7.3 – 14.5 Ra μin.


Medium Dynamic Surface Static Surface
Reciprocating Rotary
RMS  Ra μin  RMS Ra μin  RMS Ra μin 
Liquids 8 to 16 7.2 to 14.4 8 to 12 7.2 to 10.8 16 to 32

14.4 to 28.8

Plunger alignment needs to have a minimal shaft-to-bore misalignment with tight concentric guidance between the wash body and pump head. For best sealing performance, the shaft-to-bore misalignment should be kept to a minimum. 

Shaft To Bore Misalignment at the Seal Area
Shaft Diameter (in inches) Shaft to Bore Misalignment (in inches)
0.000 – 0.750 0.0020
0.751 – 1.500 0.0025
1.501 – 3.000 0.0030
3.001 – 6.000 0.0035
6.001 – 10.000 0.0045


HPLC Spring Energized Seal Recommendations

The HPLC spring energized seal requirements should be considered during the pump design process. Designers should collaborate with seal engineers early in development. Contact us today to get a quote on your next custom seal needs. 


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Spring-Energized Seals for Spaceflight

With the success of commercial spaceflight companies such as SpaceX, Blue Origin, and Virgin Galactic, there is an increasing demand for high performance, dependable seals. Rockets are one of the areas where harsh environment seals are needed, but also pose extremely challenging issues for success. Spring energized seals are one solution, but why?

What Makes a Modern Rocket

Successful spaceflight involves rockets, and the primary sections of a modern two-stage rocket are the first stage engine bay, first stage, second stage engine bay, second stage, and, last of all, the payload. This constitutes the most common configuration for today’s NewSpace companies. 

Such a configuration features an expendable or reusable first stage that contains 4 to 9 engines (the number of engines varies based on company design) and an expendable second stage that typically contains a single vacuum-optimized engine. The goal of the first and second stages is to produce enough thrust to achieve a targeted orbital velocity–usually around 17,500 mph– for the payload that sits on top of the rocket.

Propellants and Pressurants

Most rockets use either solid or liquid propellant. In this blog post, the focus will be on bi-propellant rockets, which are most commonly being used or developed in the United States commercial market. Bi-propellant rockets, as the name implies, use a combination of propellants. Common propellant configurations include:

  • RP-1 (Highly refined kerosene)/Liquid Oxygen (LOX) (aka, Kero-Lox)
  • Liquid Methane/LOX (aka, Metha-Lox or Lox-meth)
  • Liquid Hydrogen/LOX (Hydro-Lox)

Pressurants and support fluids include:

  • GN2 (Gaseous Nitrogen)
  • Helium (He)
  • GOX (Gaseous Oxygen)
  • GCH4 (Gaseous Methane)

How Modern Rocket Propulsion Systems Work

For a pump-fed system, the propellants are fed from low pressure tanks into a turbopump assembly (TPA). This significantly raises the pressures to be injected into the main combustion chamber (MCC). In most cases, a small portion of the propellants are scavenged from the high-pressure side to feed a separate small combustion chamber known as a gas-generator or pre-burner and used to drive the turbine. These fuel or oxygen rich gases can then either be vented to the atmosphere or re-injected into the MCC.

Operating Conditions of a Rocket Propulsion System

Consideration of the operating conditions within a rocket propulsion system provides insight into the challenges faced by the seals.

  • State 1 – Tank to Turbopump Assembly (TPA) inlet: propellants (oxygen + methane) are usually around 50 -150 psi and RP1 will be between 20 F and 80 F while the cryogenics will be between -450 F to -260 F.
  • State 2 – TPA outlet: depending on the engine, pumps will raise these pressures to somewhere between 1,500 and 16,000 PSI.
  • State 3 – Pre-burner: pressure will have dropped across the lines and injector – usually 8-15%, however temperatures will be between 800 -1,500 F.
  • State 4: depending on the engine cycle, propellants may be in a liquid-liquid state, gas-liquid state, or gas-gas state at an array of temperatures and pressures before mixing in the MC; note that in most cases the fluids will be supercritical.
  • State 5: once across the injector, the remaining propellants will combust at temperatures higher than 4000 F while pressure in the MCC may be between 50-20% of State 2 depending on system losses; note that this pressure drops quickly as the gases are pushed toward the atmosphere.

Depending upon which stage is involved, seal requirements vary greatly but high pressures and extreme temperatures will always be involved. 

Rocket Engine Seals

Rocket engine seals must perform in some of the most harsh environments imaginable and may involve wide operating temperature ranges (including cryogenic), extreme pressures, wide thermal cycling, and chemical compatibility with fuels, propellants, and pressurants. Most importantly, they must be extremely reliable. As an example, consider the just a rocket turbopump.

The image shown is a Hydro-Lox turbopump with a geared coupling used in the Aerojet Rocketdyne RL10 engine. Where it is labeled with a 1 indicates flange locations that likely use spring-energized face seals. Downstream of the outlets  will be the main valves, and they too will most likely have additional flange connections that will require seals. Areas labeled with 2 indicate other flange locations that depend on face seals of unknown makeup but likely involve hot gas connections.

Spring Energized Seals: A Rocket Sealing Solution

One of the most reliable, harsh environment sealing solutions is the spring energized seal. Unlike conventional seals, a spring energized seal includes an energizer that enables the seal lip to stay in contact with the mating surface through extreme variations in pressure and temperature,and  dimensional changes, as well as out of roundness, eccentricity, hardware misalignment, and some degree of wear. Vibration, cryogenic temperatures, and high temperatures are also an area where spring-energized seals offer outstanding performance.

They are highly durable in operating environments where other seals simply cannot survive. In fact, the performance of such seals has been well established in aviation and aerospace, including both NASA and commercial rockets. 

A wide variety of jacket materials are available, with some of the most widely used aerospace options being PTFE (trade name Teflon) and Hytrel. Materials such as Teflon and Hytrel can handle extreme temperatures, are chemically compatible with media involved, are heat resilient, provide low friction, have excellent wear characteristics, and are typically self lubricating. In addition, both materials are available in grades that provide key characteristics such as improved wear, lower friction, additional stiffness, better strength, etc.

And the same is true for spring energizers, which vary in both geometry and material used. For example, vacuum pressure and cryogenic applications often utilize V-springs (also known as V ribbon springs), high pressure environments may use coil springs, and vacuum pressure operating conditions with medium speeds may utilize helical springs. Various materials can be used for the spring, which will be enclosed within the seal jacket; because of this, the spring material will be protected from whatever media is being sealed.


If you are in need of spring energized seals for space applications, allow the seal specialists at Advanced EMC help you. We have a long history of providing our customers with the seals they need, including custom engineered and manufactured solutions that not only meet their specifications but also the rigorous standards that may be involved. Advanced EMC has the design, manufacturing, and testing capabilities you need to make your design a success. Contact us today to learn more.

by Sara McCaslin, PhD Sara McCaslin, PhD No Comments

PTFE Spring Energized Seals for Cryogenic Applications

When cryogenic temperatures are involved, a failed seal can have extremely serious repercussions that can include personal safety, explosions, damage to local ecosystems, and highly expensive downtime. One of the most dependable solutions to date for sealing in cryogenic environments is PTFE spring-energized seals. In this week’s blog post, we will discuss PTFE spring energized seals for cryogenic applications!

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by Sara McCaslin, PhD Sara McCaslin, PhD No Comments

Spring Energized Sealing Solutions For Cryogenic Services in LNG Plants

There are a limited number of reliable sealing solutions for cryogenic services in LNG plants, two leading polymers in use are spring-energized PTFE or UHMW seals.

Challenges of Working with LNG

Leaks involving LNG (Liquified Natural Gas) at cryogenic temperatures are dangerous to the health and safety of workers and to plant operation. Issues such as toxicity, extreme cold, asphyxiation, flammability, and explosions resulting from rapid expansion of LNG all point to the need for a reliable, leak-proof seal.

Finding an effective sealing solution for use in the cryogenic work environment of LNG plants can be extremely challenging. Keep in mind that nitrogen exists in liquid form under normal atmospheric pressure between -346°F and -320.44°F. It’s liquid to gas expansion ratio is very high at 1:694, which means as it boils (starting at its boiling point of -320.44°F) it will expand 694x its original volume. This can lead to an extremely high-pressure change if it occurs in a sealed environment, and most LNG seals must remain functional at either vacuum pressures or extremely high pressures.

Cryogenic Seals for LNG Plants

The temperatures involved with LNG happen to lie where many elastomeric and polymeric materials lose their elasticity and begin to behave as brittle materials. Some seals will also experience dimensional fluctuations related to temperature changes, further increasing the probability of failure. If temperature fluctuations are cyclical, there are going to be problems related to cyclic stress. Yet another issue related to dynamic cryogenic seals is lubrication: at such low temperatures, standard lubrication solutions simply will not work.

The Options For Sealing are Limited two either UHMW or PTFE Polymers and a Full Contact- Anti-Shrink Spring is Essential.

Both seal jacket materials can be specified PTFE, often known by its trade names Teflon or Flourolon 1000. The Ultra High Molecular Weight PE or UHMW, Fluorolon 5000 can handle the low temperatures involved in cryogenic service without becoming brittle (some grades can handle temperatures as low as -350°F) or succumb quickly to the effects of cyclical stress. In addition, both UHMW and  PTFE are self-lubricating, low friction supports dry running, and is a nonstick/slip material. In addition, both products are compatible with a wide range of chemicals, including those it would encounter in an LNG plant.

A spring-energized seal is a seal assembly that includes an energizing spring that forces the seal lip against the mating surface to achieve a highly leak-proof seal. This seal design, when combined with a PTFE lip, has been found ideal for cryogenic applications involving LNG. The spring energizer adds permanent resilience to the seal and can compensate for lip wear, eccentricity, hardware misalignment, and (perhaps most importantly when working with LNG) extreme pressures and dimensional changes. 

The recommended geometry for the spring energizer is a simple helical spring when cryogenic temperatures and either static, reciprocating, or rotary motion is involved. However, oscillatory or static motion may require the use of a solid spring. Recommended spring materials include  17-7 precipitation hardening stainless steel, 301/304 stainless steel, or, in some applications, Hastelloy, 316 stainless steel, Inconel, or Elgiloy.


The design of cryogenic seals for use in LNG plants can be challenging and must meet extremely high standards for reliability and safety, but PTFE spring-energized seals are an excellent starting point.

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Factors Influencing PTFE Seal Behavior: The Mating Surface – Part 1 in a 3 Part Series

The useful life of a PTFE seal is heavily influenced by the surface over which the seal slides or rotates. This includes both the material choice, surface finish, and hardness of the mating surface. In this article, we will look at how the mating surface influences the life and behavior of a PTFE seal and how to account for that effect during the design process.

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